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Identification of the Isomeric Dideutero p−Benzoquinones by 13C−H and 13C−D Coupling Constants

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Dabrowski,  Janusz
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Griebel,  Dieter
Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society;

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Zimmermann,  Herbert
Department of Molecular Physics, Max Planck Institute for Medical Research, Max Planck Society;
Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society;
Zimmermann Group, Max Planck Institute for Medical Research, Max Planck Society;
Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society;

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Citation

Dabrowski, J., Griebel, D., & Zimmermann, H. (1979). Identification of the Isomeric Dideutero p−Benzoquinones by 13C−H and 13C−D Coupling Constants. Spectroscopy Letters, 12(9), 661-669. doi:10.1016/0301-0104(79)85101-0.


Cite as: https://hdl.handle.net/11858/00-001M-0000-0019-B0B4-F
Abstract
2,s− and 2,6−dideuterobenzoquinone−l,4 were prepared by a direct catalytic (NaBD4/PdC12) exchange of bromine in the corresponding dibromo derivatives and the subsequent oxidation with Ag20. The structure of the products was unambiguously established by proton−carbon and deuteron−carbon splitting pattern of their NMR spectra