Specifically deuteriated intermediates for the synthesis of liquid crystals and 
liquid-crystalline polymers

Zimmermann, Herbert

doi:10.1080/02678298908033195

Item

ITEM ACTIONSEXPORT

Add to Basket

Local TagsRelease HistoryDetailsSummary

Released

Journal Article

Specifically deuteriated intermediates for the synthesis of liquid crystals and liquid-crystalline polymers

MPS-Authors

/persons/resource/persons128263

Zimmermann, Herbert
Department of Molecular Physics, Max Planck Institute for Medical Research, Max Planck Society;
Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society;
Zimmermann Group, Max Planck Institute for Medical Research, Max Planck Society;
Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society;

External Resource

http://www.tandfonline.com/doi/abs/10.1080/02678298908033195?needAccess=true#aHR0cDovL3d3dy50YW5kZm9ubGluZS5jb20vZG9pL3BkZi8xMC4xMDgwLzAyNjc4Mjk4OTA4MDMzMTk1P25lZWRBY2Nlc3M9dHJ1ZUBAQDA=
(Any fulltext)

https://doi.org/10.1080/02678298908033195
(Any fulltext)

Fulltext (restricted access)

There are currently no full texts shared for your IP range.

Fulltext (public)

There are no public fulltexts stored in PuRe

Supplementary Material (public)

There is no public supplementary material available

Citation

Zimmermann, H. (1989). Specifically deuteriated intermediates for the synthesis of liquid crystals and liquid-crystalline polymers. Liquid Crystals, 4(6), 591-618. doi:10.1080/02678298908033195.

Cite as: https://hdl.handle.net/11858/00-001M-0000-0019-ADED-3

Abstract

The recent developments in solid state N.M.R. techniques have rendered deuterium a most attractive nucleus for use in the study of liquid crystals and other ordered systems. Its application often requires that the deuterium be positioned at specific sites in the molecule. Here, the preparation of such specifically labelled compounds for use in liquid crystal research is discussed. It is shown that many deuteriated liquid crystals can be prepared from a limited set of labelled intermediates. Strategies for the labelling of such intermediates in both aromatic and aliphatic sites based on experience gained in the author's laboratory during the last years are discussed. In the experimental section more than fifty procedures for obtaining specifically deuteriated intermediates and mesogens are described in detail.