A Strategy for the Synthesis of Mesostructured Metal Oxides with Lower 
Oxidation States

Tüysüz, Harun; Weidenthaler, Claudia; Schüth, Ferdi

doi:10.1002/chem.201103650

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A Strategy for the Synthesis of Mesostructured Metal Oxides with Lower Oxidation States

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Tüysüz, Harun
Research Group Tüysüz, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Weidenthaler, Claudia
Research Group Weidenthaler, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Schüth, Ferdi
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Tüysüz, H., Weidenthaler, C., & Schüth, F. (2012). A Strategy for the Synthesis of Mesostructured Metal Oxides with Lower Oxidation States. Chemistry – A European Journal, 18(16), 5080-5086. doi:10.1002/chem.201103650.

Cite as: https://hdl.handle.net/11858/00-001M-0000-000E-748C-F

Abstract

A detailed study on the pseudomorphic conversion of ordered mesoporous Co₃O₄ and ferrihydrite into CoO and Fe₃O₄, respectively, by using alcohol/water vapor as a gentle reducing agent is described. The reduction conditions for the transformation were optimized. In addition, the first one-pot synthesis of mesostructured CoO by using nanocasting with cubic ordered silica as a hard template is demonstrated.