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Journal Article

Ethylenebis(phosphonic acid)

MPS-Authors
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Krüger,  Carl
Service Department Krüger (XRAY), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Lehmann,  Christian W.
Service Department Lehmann (EMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Leitner,  Walter
Research Group Leitner, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Rust,  Jörg
Service Department Lehmann (EMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Bruckmann, J., Krüger, C., Lehmann, C. W., Leitner, W., Rust, J., & Six, C. (1999). Ethylenebis(phosphonic acid). Acta Crystallographica, Section C: Crystal Structure Communications, 55(Part 4), 695-696. doi:10.1107/S0108270198016448.


Cite as: https://hdl.handle.net/11858/00-001M-0000-0024-6CDB-A
Abstract
The as yet structurally uncharacterized title compound,
C2H804P2, was isolated as a by-product of the synthesis
of 1,2-bis(dimethylphosphino)ethane (dmpe) from 1,2-bis(dichlorophosphino)ethane. In the crystal structure,
which is characterized by strong intermolecular O-H…Osp2 hydrogen bonds, only the R*,S* diastereomer
is found. The molecule is located on a center of inversion intersecting the central C-C bond, thereby preserving the molecular Ci symmetry.