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Journal Article

Ethylenebis(phosphonic acid)

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http://pubman.mpdl.mpg.de/cone/persons/resource/persons58723

Krüger,  C.
Service Department Krüger (XRAY), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons58744

Lehmann,  C.
Service Department Lehmann (EMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons58749

Leitner,  W.
Research Group Leitner, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons58946

Rust,  J.
Service Department Lehmann (EMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Bruckmann, J., Krüger, C., Lehmann, C., Leitner, W., Rust, J., & Six, C. (1999). Ethylenebis(phosphonic acid). Acta Crystallographica, Section C: Crystal Structure Communications, 55(Part 4), 695-696. doi:10.1107/S0108270198016448.


Cite as: http://hdl.handle.net/11858/00-001M-0000-0024-6CDB-A
Abstract
The as yet structurally uncharacterized title compound, C2H804P2, was isolated as a by-product of the synthesis of 1,2-bis(dimethylphosphino)ethane (dmpe) from 1,2-bis(dichlorophosphino)ethane. In the crystal structure, which is characterized by strong intermolecular OH…Osp2 hydrogen bonds, only the R*,S* diastereomer is found. The molecule is located on a center of inversion intersecting the central C---C bond, thereby preserving the molecular Ci symmetry.