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Kinetic 15N-CPMAS-NMR study of a double proton transfer in a crystalline malonaldehyde diimine derivative

MPG-Autoren
http://pubman.mpdl.mpg.de/cone/persons/resource/persons128263

Zimmermann,  Herbert
Department of Molecular Physics, Max Planck Institute for Medical Research, Max Planck Society;
Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society;
Zimmermann Group, Max Planck Institute for Medical Research, Max Planck Society;
Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society;

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Zitation

Limbach, H., Wehrle, B., Zimmermann, H., Kendrick, R. D., & Yannoni, C. S. (1987). Kinetic 15N-CPMAS-NMR study of a double proton transfer in a crystalline malonaldehyde diimine derivative. Angewandte Chemie, International Edition in English, 26(3), 247-248. doi:10.1002/anie.198702471.


Zitierlink: http://hdl.handle.net/11858/00-001M-0000-0019-AE85-3
Zusammenfassung
Solid state effects gave rise to an energy difference of about 4 kJ mol−1 between the tautomers 1 and 2. This could be deduced from dynamic 15N-NMR spectra, which were recorded under the conditions of cross-polarization and of sample rotation about the magic angle.