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Spark Plasma Sintering Effect on the Decomposition of MgH2

MPG-Autoren
http://pubman.mpdl.mpg.de/cone/persons/resource/persons126834

Schmidt,  J.
Max Planck Institute for Chemical Physics of Solids, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons126783

Niewa,  R.
Max Planck Institute for Chemical Physics of Solids, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons126835

Schmidt,  M.
Marcus Schmidt, Chemical Metal Science, Max Planck Institute for Chemical Physics of Solids, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons126626

Grin,  Y.
Juri Grin, Chemical Metal Science, Max Planck Institute for Chemical Physics of Solids, Max Planck Society;

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Zitation

Schmidt, J., Niewa, R., Schmidt, M., & Grin, Y. (2005). Spark Plasma Sintering Effect on the Decomposition of MgH2. Journal of the American Ceramic Society, 88(7), 1870-1874. doi:10.1111/j.1551-2916.2005.00358.x.


Zitierlink: http://hdl.handle.net/11858/00-001M-0000-0015-2CA7-A
Zusammenfassung
Spark plasma sintering (SPS) is one of the advanced consolidation techniques developed in the last few decades. We have studied the decomposition behavior of MgH2 and MgH2/graphite 1:1 mixtures in the SPS process. The standard SPS setup chosen was modified by including the temperature measurement inside the sample, so that the data can be compared with findings from thermal analysis. The results show clearly the reduction of the decomposition temperature measured in the SPS process if the necessary conditions (sufficient current density by applying the insulation) are realized.