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Diffraction and Spectroscopy of Porous Solids

MPS-Authors
http://pubman.mpdl.mpg.de/cone/persons/resource/persons58966

Schmidt,  W.
Research Group Schmidt, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons58985

Schüth,  Ferdi
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons59100

Weidenthaler,  Claudia
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Schmidt, W., Schüth, F., & Weidenthaler, C. (2013). Diffraction and Spectroscopy of Porous Solids. In Reference Module in Chemistry, Molecular Sciences and Chemical Engineering Comprehensive Inorganic Chemistry II (Second Edition) From Elements to Applications Volume 5: Porous Materials and Nanomaterials (pp. 1-24).


Cite as: http://hdl.handle.net/11858/00-001M-0000-0014-A2E8-D
Abstract
Porous solids are in the first place solids and thus all methods for the analysis of common solids can be also applied on porous ones. Structural information and bulk properties of the solid are accessible as for any other material. In addition, specific information on pore sizes, pore shapes, and properties of pore surfaces of such material can be obtained by different methods as well as information on guest species within the pores and on host–guest interactions. In the present chapter, diffraction and spectroscopic methods for the analysis of porous solids will be described and the type of information that can be achieved by the different methods will be illustrated. Diffraction and scattering of x-rays, neutrons, and electrons by a porous solid will be introduced as well as the application of infrared and nuclear magnetic resonance spectroscopy for the analysis of surface properties, host–guest interaction, and diffusion studies that are complemented by interference microscopy.