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Application of an eremomycin-chiral stationary phase for the separation of DL-methionine using simulated moving bed technology

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http://pubman.mpdl.mpg.de/cone/persons/resource/persons86529

Zhang,  L.
Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons86301

Gedicke,  K.
Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons86477

Seidel-Morgenstern,  A.
Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society;
Otto-von-Guericke-Universität Magdeburg, External Organizations;

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Citation

Zhang, L., Gedicke, K., Kuznetsov, M. A., Staroverov, S. M., & Seidel-Morgenstern, A. (2007). Application of an eremomycin-chiral stationary phase for the separation of DL-methionine using simulated moving bed technology. Journal of Chromatography A, 1162, 90-96. doi:10.1016/j.chroma.2007.04.033.


Cite as: http://hdl.handle.net/11858/00-001M-0000-0013-98BE-D
Abstract
Recently a new chiral stationary phase (CSP) was introduced, based on the immobilization of the macrocyclic glycopeptide eremomycin to epoxy-activated silica. The application of this new CSP to preparative enantioseparation using simulated moving bed chromatography (SMB) will be presented. In such delicate continuous separation processes, besides selectivity, the long-term stability of the applied stationary phases is of importance. Column to column fluctuations of the bed homogeneity and long-term stability of the preparative stationary phase was satisfactory according to the results of perturbation experiments performed before and after long-term SMB runs. Copyright © 2007 Elsevier B.V. All rights reserved. [accessed 2013 November 26th]