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Experimental validation of a new integrated simulated moving bed process for the production of single enantiomers

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http://pubman.mpdl.mpg.de/cone/persons/resource/persons86300

García Palacios,  J.
Process Synthesis and Process Dynamics, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society;
International Max Planck Research School (IMPRS), Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons86194

Kramer,  Bernhard
Analysis and Redesign of Biological Networks, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons86359

Kienle,  A.
Process Synthesis and Process Dynamics, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society;
Otto-von-Guericke-Universität Magdeburg, External Organizations;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons86349

Kaspereit,  M.
Process Synthesis and Process Dynamics, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society;

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Citation

García Palacios, J., Kramer, B., Kienle, A., & Kaspereit, M. (2011). Experimental validation of a new integrated simulated moving bed process for the production of single enantiomers. Journal of Chromatography A, 2218(16), 2232-2239. doi:10.1016/j.chroma.2011.02.021.


Cite as: http://hdl.handle.net/11858/00-001M-0000-0013-8D0C-7
Abstract
A new integrated 3-zone simulated moving bed (SMB) concept with internal racemization reaction was suggested recently for the production of single enantiomers from racemic mixtures [1,2]. The process utilizes an internal gradient to trigger the racemization within a single zone. It can deliver the pure enantiomer and outperforms conventional technologies. In this contribution, the concept is validated experimentally for the separation of a model system compound. The results demonstrate that the new concept is capable of producing a single enantiomer with purity, yield and conversion of 100%. © 2011 Elsevier B.V. All rights reserved. [accessed 2013 July 2nd]