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A Strategy for the Synthesis of Mesostructured Metal Oxides with Lower Oxidation States

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http://pubman.mpdl.mpg.de/cone/persons/resource/persons59060

Tüysüz,  Harun
Research Group Tüysüz, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons59100

Weidenthaler,  Claudia
Research Group Weidenthaler, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

http://pubman.mpdl.mpg.de/cone/persons/resource/persons58985

Schüth,  Ferdi
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Tüysüz, H., Weidenthaler, C., & Schüth, F. (2012). A Strategy for the Synthesis of Mesostructured Metal Oxides with Lower Oxidation States. Chemistry – A European Journal, 18(16), 5080-5086. doi:10.1002/chem.201103650.


Cite as: http://hdl.handle.net/11858/00-001M-0000-000E-748C-F
Abstract
A detailed study on the pseudomorphic conversion of ordered mesoporous Co3O4 and ferrihydrite into CoO and Fe3O4, respectively, by using alcohol/water vapor as a gentle reducing agent is described. The reduction conditions for the transformation were optimized. In addition, the first one-pot synthesis of mesostructured CoO by using nanocasting with cubic ordered silica as a hard template is demonstrated.