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  Continuous flow processes for photoconjugation of high-molecular chemical entities

Seeberger, P. H., Laurino, P., Kikkeri, R., O'Brien, A. G., Klein, J. C., & Götze, S.(2012). Continuous flow processes for photoconjugation of high-molecular chemical entities.

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 Urheber:
Seeberger, Peter H.1, Autor           
Laurino, P.2, Autor           
Kikkeri, R.2, Autor           
O'Brien, Alexander G.2, Autor           
Klein, James C.2, Autor           
Götze, Sebastian3, Autor           
Affiliations:
1Peter H. Seeberger - Automated Systems, Biomolekulare Systeme, Max Planck Institute of Colloids and Interfaces, Max Planck Society, ou_1863306              
2Biomolekulare Systeme, Max Planck Institute of Colloids and Interfaces, Max Planck Society, ou_1863286              
3Daniel Varón Silva, Biomolekulare Systeme, Max Planck Institute of Colloids and Interfaces, Max Planck Society, ou_1863302              

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 Zusammenfassung: The invention relates to a continuous flow process for the photoconjugation of chemical entities selected from the group comprising carbohydrates, including mono-, oligo- and polysaccharides, amino acids, peptides and proteins, unbranched and branched oligomers and polymers, including dendrimers, which process comprises at least the following steps: a) providing a mixture of the reactants dissolved in an aqueous or organic solvent; b) passing said mixture through a continuous flow reactor and concomitantly irradiating the mixture with light in order to initiate and perform the photoreaction. In preferred embodiments, the photoconjugation is a thiol-ene conjugation or a [2+2] cycloaddition. A further aspect of the invention relates to the conjugates obtainable by this continuous flow process, in particular dendronized polymers such as carbohydrate-dendronized polymers.

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 Datum: 2011-11-232012-05-31
 Publikationsstatus: Online veröffentlicht
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 Identifikatoren: Patentpublikationsnr.: WO2013139803 A1
Patentantragsnr.: PCT/EP2011/005898
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