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  Heteronuclear dipolar recoupling in liquid crystals and solids by PISEMA-type pulse sequences

Dvinskikh, S. V., Zimmermann, H., Maliniak, A., & Sandström, D. (2003). Heteronuclear dipolar recoupling in liquid crystals and solids by PISEMA-type pulse sequences. Journal of Magnetic Resonance, 164(1), 165-170. doi:10.1016/S1090-7807(03)00180-0.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0029-ACC6-6 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-0029-ACC7-4
Genre: Journal Article
Alternative Title : Heteronuclear dipolar recoupling in liquid crystals and solids by PISEMA-type pulse sequences

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JMagnReson_164_2003_165.pdf (Any fulltext), 138KB
 
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 Creators:
Dvinskikh, Sergey V., Author
Zimmermann, Herbert1, 2, Author           
Maliniak, Arnold, Author
Sandström, Dick, Author
Affiliations:
1Department of Molecular Physics, Max Planck Institute for Medical Research, Max Planck Society, ou_1497705              
2Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society, ou_1497700              

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Free keywords: Heteronuclear recoupling; Magic-angle spinning; Cross-polarization; PISEMA; Liquid crystals
 Abstract: A pulse sequence is described for the recoupling of heteronuclear dipolar interactions under MAS. The method is similar to the PISEMA experiment, but employs a well-defined amplitude modulation of one of the two radio-frequency fields. The technique is used for measurements of 1H-13C dipolar couplings in unoriented solid and liquid-crystalline samples.

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Language(s): eng - English
 Dates: 2003-05-092003-03-102003-07-012003-09-01
 Publication Status: Issued
 Pages: 6
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: eDoc: 665878
DOI: 10.1016/S1090-7807(03)00180-0
URI: http://www.ncbi.nlm.nih.gov/pubmed/12932469
URI: http://dx.doi.org/10.1016/S1090-7807(03)00180-0
Other: 5991
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Title: Journal of Magnetic Resonance
Source Genre: Journal
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Publ. Info: San Diego [etc.] : Academic Press
Pages: - Volume / Issue: 164 (1) Sequence Number: - Start / End Page: 165 - 170 Identifier: ISSN: 0022-2364
CoNE: https://pure.mpg.de/cone/journals/resource/954922651175_1