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  The Phase Behavior and Crystallization of 2-Chloromandelic Acid: The Crystal Structure of the Pure Enantiomer and the Behavior of Its Metastable Conglomerate

Lorenz, H., von Langermann, J., Sadiq, G., Seaton, C. C., Davey, R. J., & Seidel-Morgenstern, A. (2011). The Phase Behavior and Crystallization of 2-Chloromandelic Acid: The Crystal Structure of the Pure Enantiomer and the Behavior of Its Metastable Conglomerate. Crystal Growth & Design, 11(5), 1549-1556. doi:10.1021/cg1015077.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0013-8D16-F Version Permalink: https://hdl.handle.net/11858/00-001M-0000-0014-B3E9-6
Genre: Journal Article

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 Creators:
Lorenz, H.1, Author           
von Langermann, J.1, Author           
Sadiq, G.2, Author
Seaton, C. C.2, Author
Davey, R. J.2, Author
Seidel-Morgenstern, A.1, 3, Author           
Affiliations:
1Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738150              
2University of Manchester,Colloids, Crystals and Interfaces Group, School of Chemical Engineering and Analytical Science, Sackville Street, P.O. Box 88, Manchester, M60 1QD, United Kingdom, ou_persistent22              
3Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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 Abstract: Crystallization of racemic 2-chloromandelic acid yields a metastable conglomerate in addition to a more stable racemic compound. The crystal structure of the pure enantiomer is reported and the relative stability of the racemic compound and conglomerate was determined at both room temperature and the melting point. Crystallizations from melt and solution are shown to offer potential crystallization pathways to the conglomerate, provided crystallization of the racemic compound can be avoided. Copyright © 2011 American Chemical Society [accessed 27th May 2011]

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Language(s): eng - English
 Dates: 2011
 Publication Status: Issued
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: eDoc: 562224
Other: 40/11
DOI: 10.1021/cg1015077
 Degree: -

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Title: Crystal Growth & Design
Source Genre: Journal
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Publ. Info: Washington, DC : American Chemical Society
Pages: - Volume / Issue: 11 (5) Sequence Number: - Start / End Page: 1549 - 1556 Identifier: ISSN: 1528-7483
CoNE: https://pure.mpg.de/cone/journals/resource/110978984570353