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Abstract:
Direct fluorination of cyclic 1,3-diones gives 2-mono- and
2,2-di-fluorinated products. The monofluorinated compounds crystallise
in their enol forms and the difluorinated compounds form stable
monohydrates whose crystal structures have been elucidated, Direct
fluorination of phloroglucinol double dagger in formic acid yields
1,1,3,3,5,5-hexafluoro-2,2,4,4,6,6-hexahydroxtcyclohexane.