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  Synthesis and X-ray structures of tetralithium derivatives oftert-butylcalix[4]arene containing unique Li–O cores basedon a square-pyramidal geometry

Davidson, M., Howard, J., Lamb, S., & Lehmann, C. (1997). Synthesis and X-ray structures of tetralithium derivatives oftert-butylcalix[4]arene containing unique Li–O cores basedon a square-pyramidal geometry. Chemical Communications, (17), 1607-1608. doi:10.1039/A702280H.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0024-76AA-7 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-0024-76AB-5
Genre: Journal Article

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 Creators:
Davidson, M.G.1, Author
Howard, J.A.K.1, Author
Lamb, S.1, Author
Lehmann, C.W.1, 2, Author           
Affiliations:
1University of Durham, Department of Chemistry, Science Laboratories, Durham, UK DH1 3LE, ou_persistent22              
2Service Department Lehmann (EMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445625              

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 Abstract: Tetralithiation of tert-butylcalix[4]arene in the presence of hmpa (hexamethylphosphoramide) results in the isolation of either a monomeric complex in which LiOH is incorporated into an Li5O5 core based on an isolated square pyramid of Li atoms, or a dimeric LiOH-free species containing an Li8O8 core in which the same structural motif is maintained by edge-sharing of two square pyramids of Li atoms.

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Language(s): eng - English
 Dates: 1997
 Publication Status: Issued
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1039/A702280H
 Degree: -

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Title: Chemical Communications
  Other : Chem. Commun.
Source Genre: Journal
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Publ. Info: Cambridge, UK : Royal Society of Chemistry
Pages: - Volume / Issue: (17) Sequence Number: - Start / End Page: 1607 - 1608 Identifier: ISSN: 1359-7345
CoNE: https://pure.mpg.de/cone/journals/resource/954928495413