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  Particle shape optimization by changing from an isotropic to an anisotropic nanostructure: preparation of highly active and stable supported Pt catalysts in microemulsions

Parapat, R. Y., Wijaya, M., Schwarze, M., Selve, S., Willinger, M. G., & Schomäcker, R. (2013). Particle shape optimization by changing from an isotropic to an anisotropic nanostructure: preparation of highly active and stable supported Pt catalysts in microemulsions. Nanoscale, 5(2), 796-805. doi:10.1039/C2NR32122J.

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 Urheber:
Parapat, Riny Y.1, Autor
Wijaya, Muliany1, Autor
Schwarze, Michael1, Autor
Selve, Sören1, Autor
Willinger, Marc Georg2, Autor           
Schomäcker, Reinhard1, Autor
Affiliations:
1Technische Universität Berlin, Strasse des 17. Juni 124, 10623 Berlin, Germany , ou_persistent22              
2Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              

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 Zusammenfassung: We recently introduced a new method to synthesize an active and stable Pt catalyst, namely thermo-destabilization of microemulsions (see R. Y. Parapat, V. Parwoto, M. Schwarze, B. Zhang, D. S. Su and R. Schomäcker, J. Mater. Chem., 2012, 22 (23), 11605–11614). We are able to produce Pt nanocrystals with a small size (2.5 nm) of an isotropic structure i.e. truncated octahedral and deposit them well on support materials. Although we have obtained good results, the performance of the catalyst still needed to be improved and optimized. We followed the strategy to retain the small size but change the shape to an anisotropic structure of Pt nanocrystals which produces more active sites by means of a weaker reducing agent. We found that our catalysts are more active than those we reported before and even show the potential to be applied in a challenging reaction such as hydrogenation of levulinic acid.

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Sprache(n): eng - English
 Datum: 2012-08-022012-11-252012-11-272013-01-21
 Publikationsstatus: Erschienen
 Seiten: 10
 Ort, Verlag, Ausgabe: -
 Inhaltsverzeichnis: -
 Art der Begutachtung: Expertenbegutachtung
 Identifikatoren: DOI: 10.1039/C2NR32122J
 Art des Abschluß: -

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Titel: Nanoscale
Genre der Quelle: Zeitschrift
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Ort, Verlag, Ausgabe: Cambridge, UK : Royal Society of Chemistry
Seiten: - Band / Heft: 5 (2) Artikelnummer: - Start- / Endseite: 796 - 805 Identifikator: ISSN: 2040-3364
CoNE: https://pure.mpg.de/cone/journals/resource/2040-3364