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  Solubility of Mandelic Acid Enantiomers and Their Mixtures in Three Chiral Solvents

Tulashie, S. K., Lorenz, H., & Seidel-Morgenstern, A. (2010). Solubility of Mandelic Acid Enantiomers and Their Mixtures in Three Chiral Solvents. Journal of Chemical and Engineering Data, 55(11), 5196-5200. doi:10.1021/je1006955.

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Tulashie, S. K.1, Autor           
Lorenz, H.1, Autor           
Seidel-Morgenstern, A.1, 2, Autor           
Affiliations:
1Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738150              
2Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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 Zusammenfassung: A systematic study of the ternary solubility phase diagrams of chiral mandelic acid species in the chiral solvents (S)-methyl lactate, (S)-propyl lactate, and (S)-butyl lactate has been carried out. Solubility measurements were performed for different enantiomeric compositions in a temperature range between (273 and 318) K. Experimental results indicated no proof of solubility differences of the enantiomers in all three chiral solvents used. Hence, increasing chain length of the chiral solvents has no influence on chiral recognition. Besides, the eutectic composition in the chiral system in the presence of the solvent as a significant parameter for enantioseparation was determined for all the chiral solvents investigated. Also, the activity coefficients were derived for all three chiral solvents applied. copyright 2010 American Chemical Society [accessed November 18th, 2010]

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Sprache(n): eng - English
 Datum: 2010
 Publikationsstatus: Erschienen
 Seiten: -
 Ort, Verlag, Ausgabe: -
 Inhaltsverzeichnis: -
 Art der Begutachtung: Expertenbegutachtung
 Identifikatoren: eDoc: 499533
Anderer: 32/10
DOI: 10.1021/je1006955
 Art des Abschluß: -

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Titel: Journal of Chemical and Engineering Data
Genre der Quelle: Zeitschrift
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Ort, Verlag, Ausgabe: Washington : American Chemical Society
Seiten: - Band / Heft: 55 (11) Artikelnummer: - Start- / Endseite: 5196 - 5200 Identifikator: ISSN: 0021-9568
CoNE: https://pure.mpg.de/cone/journals/resource/991042728182784