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  Parametric study of thermal effects in reactive liquid chromatography

Javeed, S., Qamar, S., Seidel-Morgenstern, A., & Warnecke, G. (2012). Parametric study of thermal effects in reactive liquid chromatography. Chemical Engineering Journal, 191, 426-440. doi:10.1016/j.cej.2012.02.040.

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Javeed, S.1, 2, Autor           
Qamar, S.2, 3, Autor           
Seidel-Morgenstern, A.2, 4, Autor           
Warnecke, G.4, Autor
Affiliations:
1International Max Planck Research School (IMPRS), Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738143              
2Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738150              
3COMSATS Institute of Information Technology, Dep. of Mathematics, Islamabad, Pakistan, persistent:22              
4Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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Schlagwörter: Non-linear reactive chromatography; Parametric study of thermal effects; Convection–diffusion-reaction model; Finite volume scheme
 Zusammenfassung: This work is focused on modeling and simulation of non-isothermal reactive liquid chromatography. The model is formed by a system of convection–diffusion-reaction partial differential equations. The simulation of non-isothermal reactive chromatography is generally a challenging task for a numerical scheme due to the nonlinearity of the convection-dominated mass and energy balance equations and because of stiffness of the reaction terms. A high resolution finite volume scheme, recently developed for isothermal chromatography, is extended to solve the non-isothermal processes. The scheme is robust and gives high order accuracy on coarse grids, resolves sharp discontinuities, and avoids numerical dispersion which may lead to incorrect solutions. Although, thermal effects are typically neglected, the results of systematic parametric studies demonstrate that temperature gradients can significantly influence conversion and separation in reactive liquid chromatography. To validate the results, several consistency tests are carried out. The results prove the accuracy of the numerical scheme and quantify the relevant thermal effects. Copyright © 2012 Elsevier B.V. All rights reserved [accessed September 6th 2012]

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Sprache(n): eng - English
 Datum: 2012
 Publikationsstatus: Erschienen
 Seiten: -
 Ort, Verlag, Ausgabe: -
 Inhaltsverzeichnis: -
 Art der Begutachtung: Expertenbegutachtung
 Identifikatoren: eDoc: 609987
DOI: 10.1016/j.cej.2012.02.040
Anderer: 33/12
 Art des Abschluß: -

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Titel: Chemical Engineering Journal
Genre der Quelle: Zeitschrift
 Urheber:
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Ort, Verlag, Ausgabe: Lausanne : Elsevier
Seiten: - Band / Heft: 191 Artikelnummer: - Start- / Endseite: 426 - 440 Identifikator: ISSN: 1385-8947
CoNE: https://pure.mpg.de/cone/journals/resource/954925622211