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  Collision cross sections of high-mannose N-glycans in commonly observed adduct states – identification of gas-phase conformers unique to [M − H]- ions

Struwe, W. B., Benesch, J. L., Harvey, D. J., & Pagel, K. (2015). Collision cross sections of high-mannose N-glycans in commonly observed adduct states – identification of gas-phase conformers unique to [M − H]- ions. Analyst, 140(20), 6799-6803. doi:10.1039/C5AN01092F.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0027-F469-C Version Permalink: https://hdl.handle.net/11858/00-001M-0000-002C-AB7F-B
Genre: Journal Article

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c5an01092f-1.pdf (Publisher version), 2MB
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 Creators:
Struwe, W. B.1, Author
Benesch, J. L.1, Author
Harvey, D. J.2, Author
Pagel, Kevin3, 4, Author           
Affiliations:
1Department of Chemistry, University of Oxford, Oxford, UK, ou_persistent22              
2Department of Biochemistry, Oxford Glycobiology Institute, University of Oxford, Oxford, UK, ou_persistent22              
3Molecular Physics, Fritz Haber Institute, Max Planck Society, ou_634545              
4Institut für Chemie und Biochemie der Freien Universität Berlin, Takustr. 3, 14195 Berlin, Germany , ou_persistent22              

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 Abstract: We report collision cross sections (CCS) of high-mannose N-glycans as [M + Na]+, [M + K]+, [M + H]+, [M + Cl]-, [M + H2PO4]- and [M − H]- ions, measured by drift tube (DT) ion mobility-mass spectrometry (IM-MS) in helium and nitrogen gases. Further analysis using traveling wave (TW) IM-MS reveal the existence of distinct conformers exclusive to [M − H]- ions.

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Language(s): eng - English
 Dates: 2015-06-012015-07-062015-07-072015-10-21
 Publication Status: Issued
 Pages: 5
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1039/C5AN01092F
 Degree: -

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Title: Analyst
Source Genre: Journal
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Publ. Info: London : Royal Society of Chemistry
Pages: - Volume / Issue: 140 (20) Sequence Number: - Start / End Page: 6799 - 6803 Identifier: ISSN: 0003-2654
CoNE: https://pure.mpg.de/cone/journals/resource/954925263181